HCID 20991136, compound → HCID 20984892, compound

HRID 2375838Notes

Reaction equation

HRID 2375838 reaction equation
CC(C)(CN1CCCCC1)C(O)=O.[CH3:14][C:15]([CH3:34])([CH2:26][N:27]1[CH2:32][CH2:31][N:30]([CH3:33])[CH2:29][CH2:28]1)[C:16]([O:18]CC1C=CC=CC=1)=[O:17]>>[CH3:14][C:15]([CH3:34])([CH2:26][N:27]1[CH2:28][CH2:29][N:30]([CH3:33])[CH2:31][CH2:32]1)[C:16]([OH:18])=[O:17]

Participants

3

Reactant 2

HCID 20991136HCID 20991136, compoundHCID 58710079Phenylmethyl α,α,4-trimethyl-1-piperazinepropanoate

Product 1

HCID 20984892HCID 20984892, compound

Procedure

The procedure for 2,2-dimethyl-3-piperidin-1-ylpropanoic acid was followed except for replacing benzyl-2,2-dimethyl-3-piperidin-1-ylpropanoate with benzyl 2,2-dimethyl-3-(4-methylpiperazin-1-yl)propanoate. The compound was obtained as a yellow solid. 1H NMR (400 MHz, CDCl3): δ=1.24 (s, 6H), 2.33 (s, 3H), 2.44-2.92 (m, 10H).

Workup

  1. customThe compound was obtained as a yellow solid

Sources & evidence

ORD record
ord-f5a56d3c62094a5e9a262a00f4082c91
Source dataset
uspto-grants-2008_12
Patent number
US07465726B2

Reaction notes

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