Phenethylamine → HCID 23797016, compound

Participants

Reaction Steps

The title compound was prepared following the procedure for N,N-dimethyl-N′-(6-nitrobenzothiazol-2-yl)-ethane-1,2-diamine, using 4 eq of phenethylamine. Modified workup: Solid that had precipitated during course of reaction (amine salt) was filtered; no aqueous workup was conducted. 1H NMR (400 MHz, CDCl3): δ=3.03 (t, J=6.4 Hz, 3H), 3.77 (q, J=6.4 Hz, 2H), 7.23-7.30 (m, 3H), 7.33-7.38 (m, 2H), 7.52 (d, J=8.8 Hz, 1H), 8.21 (dd, J=8.8, 2.4 Hz, 1H), 8.51 (d, J=2.4 Hz, 1H). MS (ES+): m/z 300.10 [MH+]. HPLC: tR=3.57 min (ZQ2000, polar—5 min).

Provenance & Evidence