2-Methoxyethylamine → HCID 58710031, compound

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Reaction Steps

The title compound was prepared following the procedure for N,N-dimethyl-N′-(6-nitrobenzothiazol-2-yl)-ethane-1,2-diamine, using 6.78 eq of 2-methoxyethylamine. 1H NMR (400 MHz, CDCl3): δ=3.42 (s, 3H), 3.65 (td, J=4.4, 0.8 Hz, 2H), 3.70 (t, br, J=4.4 Hz, 2H), 5.92 (s, br, —NH), 7.53 (d, J=8.8 Hz, 1H), 8.21 (dd, J=9.2, 2.4 Hz, 1H), 8.51 (d, J=2.4 Hz, 1H). MS (ES+): m/z 254.10 (100) [MH+]. HPLC: tR=2.89 min (ZQ2000, polar—5 min).

Provenance & Evidence