HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68960778, compound → HCID 86095761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68960778 | HCID 68960778 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86095761 | HCID 86095761 | 84.2% |
Reaction Steps
A mixture of {6-[(1-benzyl-4-piperidyl)amino]-3-pyridyl}methanol (670 mg) and MnO2 (2.94 g) in AcOEt (30 ml) was refluxed under stirring for 2 hours. After removal of the insoluble material, and the solvent was evaporated in vacuo to give 6-[(1-benzyl-4-piperidyl)amino]nicotinaldehyde (560 mg)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465731B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-718a7b9810a44996a1fdf28e9f3d3fe3 |
| Source note | uspto-grants-2008_12 |