3,5-Dimethylphenol → HCID 68707816, compound

HRID 2376261Notes

Reaction equation

HRID 2376261 reaction equation
O[CH:2]([C:6]1[CH:11]=[CH:10][C:9]([CH:12]([CH3:14])[CH3:13])=[CH:8][CH:7]=1)[C:3]([OH:5])=[O:4].[CH3:15][C:16]1[CH:17]=[C:18](O)[CH:19]=[C:20]([CH3:22])[CH:21]=1>C(OCC)(=O)C.CCCCCC>[CH:12]([C:9]1[CH:10]=[CH:11][C:6]([CH:2]2[C:17]3[C:16]([CH3:15])=[CH:21][C:20]([CH3:22])=[CH:19][C:18]=3[O:5][C:3]2=[O:4])=[CH:7][CH:8]=1)([CH3:14])[CH3:13]

Participants

4

Reactant 2

HCID 79483,5-DimethylphenolHCID 23423233Hydroxy(4-isopropylphenyl)acetic acid

Product 1

HCID 68707816HCID 68707816, compoundYield 45%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using hydroxy(4-isopropylphenyl)acetic acid synthesized in Reference Example 1 and 3,5-dimethylphenol, the title compound was synthesized in the same manner as in Reference Example 2. Yield 45%. Melting point: 76-77° C. (ethyl acetate-hexane).

Sources & evidence

ORD record
ord-7cc25a875128445f8ae0a3855ea9bb1a
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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