HCID 68710223, compound → HCID 23114062, compound

HRID 2376264Notes

Reaction equation

HRID 2376264 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH:10]2[C:14]3[CH:15]=[CH:16][C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][C:11]2=[O:21])=[CH:6][CH:5]=1)([CH3:3])[CH3:2]>C(OCC)(=O)C.CCCCCC>[OH:21][CH2:11][CH:10]([C:14]1[C:13]([OH:12])=[C:18]([CH3:19])[C:17]([CH3:20])=[CH:16][CH:15]=1)[C:7]1[CH:6]=[CH:5][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:9][CH:8]=1

Participants

3

Reactant 1

HCID 68710223HCID 68710223, compound

Product 1

HCID 23114062HCID 23114062, compoundYield 36%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 3-(4-isopropylphenyl)-6,7-dimethyl-1-benzofuran-2 (3H)-one synthesized in Reference Example 3, the title compound was synthesized in the same manner as in Reference Example 8. Yield 36%. Melting point: 83-84° C. (ethyl acetate-hexane).

Workup

  1. customsynthesized in Reference Example 3

Sources & evidence

ORD record
ord-879d7a32f82845ab88ae6b80f1a34915
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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