HCID 68707816, compound → HCID 23114273, compound

HRID 2376265Notes

Reaction equation

HRID 2376265 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH:10]2[C:14]3[C:15]([CH3:20])=[CH:16][C:17]([CH3:19])=[CH:18][C:13]=3[O:12][C:11]2=[O:21])=[CH:6][CH:5]=1)([CH3:3])[CH3:2]>C(OCC)(=O)C.CCCCCC>[OH:21][CH2:11][CH:10]([C:14]1[C:15]([CH3:20])=[CH:16][C:17]([CH3:19])=[CH:18][C:13]=1[OH:12])[C:7]1[CH:6]=[CH:5][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:9][CH:8]=1

Participants

3

Reactant 1

HCID 68707816HCID 68707816, compound

Product 1

HCID 23114273HCID 23114273, compoundYield 93%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 3-(4-isopropylphenyl)-4,6-dimethyl-1-benzofuran-2 (3H)-one synthesized in Reference Example 4, the title compound was synthesized in the same manner as in Reference Example 8. Yield 93%. Melting point: 101-102° C. (ethyl acetate-hexane).

Workup

  1. customsynthesized in Reference Example 4

Sources & evidence

ORD record
ord-edc413c89b254d1789e820104e78ef09
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

Loading…