HCID 23114062, compound → HCID 23114082, compound

HRID 2376268Notes

Reaction equation

HRID 2376268 reaction equation
O[CH2:2][CH:3]([C:13]1[C:18]([OH:19])=[C:17]([CH3:20])[C:16]([CH3:21])=[CH:15][CH:14]=1)[C:4]1[CH:9]=[CH:8][C:7]([CH:10]([CH3:12])[CH3:11])=[CH:6][CH:5]=1>CO>[CH:10]([C:7]1[CH:8]=[CH:9][C:4]([CH:3]2[C:13]3[CH:14]=[CH:15][C:16]([CH3:21])=[C:17]([CH3:20])[C:18]=3[O:19][CH2:2]2)=[CH:5][CH:6]=1)([CH3:12])[CH3:11]

Participants

3

Reactant 1

HCID 23114062HCID 23114062, compound

Product 1

HCID 23114082HCID 23114082, compoundYield 80%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Using 6-(2-hydroxy-1-(4-isopropylphenyl)ethyl)-2,3-dimethylphenol synthesized in Reference Example 9, the title compound was synthesized in the same manner as in Reference Example 13. Yield 80%. Melting point: 50-51° C. (methanol).

Workup

  1. customsynthesized in Reference Example 9

Sources & evidence

ORD record
ord-7d95a14d343c4099acb76de1bdd3f01d
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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