HCID 23114273, compound → HCID 23114042, compound

HRID 2376269Notes

Reaction equation

HRID 2376269 reaction equation
[OH:1][CH2:2][CH:3]([C:13]1[C:18]([CH3:19])=[CH:17][C:16]([CH3:20])=[CH:15][C:14]=1O)[C:4]1[CH:9]=[CH:8][C:7]([CH:10]([CH3:12])[CH3:11])=[CH:6][CH:5]=1>CO>[CH:10]([C:7]1[CH:6]=[CH:5][C:4]([CH:3]2[C:13]3[C:18]([CH3:19])=[CH:17][C:16]([CH3:20])=[CH:15][C:14]=3[O:1][CH2:2]2)=[CH:9][CH:8]=1)([CH3:12])[CH3:11]

Participants

3

Reactant 1

HCID 23114273HCID 23114273, compound

Product 1

HCID 23114042HCID 23114042, compoundYield 85%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Using 2-(2-hydroxy-1-(4-isopropylphenyl)ethyl)-3,5-dimethylphenol synthesized in Reference Example 10, the title compound was synthesized in the same manner as in Reference Example 13. Yield 85%. Melting point: 46-47° C. (methanol).

Workup

  1. customsynthesized in Reference Example 10

Sources & evidence

ORD record
ord-dc61c8ed694c4c629c570315213ed288
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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