2,5-Dimethylphenol → HCID 17605963, compound
Reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([CH3:8])=[CH:4][C:3]=1[OH:9].[C:10]([O:13]CC)(=[O:12])C.CCC[CH2:19][CH2:20][CH3:21]>>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([CH3:8])=[CH:4][C:3]=1[O:9][C:20]([CH3:19])([CH3:21])[C:10]([OH:13])=[O:12]Participants
3
Procedure
Using 2,5-dimethylphenol, the title compound was synthesized in the same manner as in Reference Example 36. Yield 57%. Melting point: 107-109° C. (ethyl acetate-hexane).
Sources & evidence
- ORD record
- ord-64e046a1a36a4b2b99fb9b1393f2aa2d
- Source dataset
- uspto-grants-2008_12
- Patent number
- US07465815B2
Reaction notes
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