3-Pyridinylboronic acid → HCID 86697301, compound

HRID 237628Notes

Reaction equation

HRID 237628 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3](B(O)O)[CH:2]=1.[Br:10][C:11]1[C:16]([CH3:17])=[CH:15][C:14](I)=[CH:13][C:12]=1[CH3:19]>>[Br:10][C:11]1[C:16]([CH3:17])=[CH:15][C:14]([C:3]2[CH:2]=[N:1][CH:6]=[CH:5][CH:4]=2)=[CH:13][C:12]=1[CH3:19]

Participants

3

Reactant 2

HCID 27343783-Pyridinylboronic acidHCID 207480372-Bromo-5-iodo-1,3-dimethylbenzene

Product 1

HCID 86697301HCID 86697301, compound

Procedure

The title compound is prepared from pyridine-3-boronic acid and 2-bromo-5-iodo-1,3-dimethyl-benzene following a procedure analogous to that described in Step 1 of Intermediate 56. LC (method 9): tR=0.99 min; Mass spectrum (ESI+): m/z=262/264 (Br) [M+H]+.

Sources & evidence

ORD record
ord-df68dd4c252247ad88435d048c628c3a
Source dataset
uspto-grants-2014_02
Patent number
US08642585B2

Reaction notes

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