HCID 23114252, compound → HCID 23114203, compound

HRID 2376284Notes

Reaction equation

HRID 2376284 reaction equation
[CH3:1][C:2]1([CH3:17])[C:6](=[O:7])[C:5]2[C:8]([CH3:16])=[C:9]([N+:13]([O-])=O)[CH:10]=[C:11]([CH3:12])[C:4]=2[O:3]1>C(OCC)(=O)C.CCCCCC>[NH2:13][C:9]1[CH:10]=[C:11]([CH3:12])[C:4]2[O:3][C:2]([CH3:1])([CH3:17])[C:6](=[O:7])[C:5]=2[C:8]=1[CH3:16]

Participants

3

Reactant 1

HCID 23114252HCID 23114252, compound

Product 1

HCID 23114203HCID 23114203, compoundYield 97%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 2,2,4,7-tetramethyl-5-nitro-1-benzofuran-3 (2H)-one obtained in Reference Example 47, the title compound was synthesized in the same manner as in Reference Example 54. Yield 97%. Melting point: 124-126° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 47

Sources & evidence

ORD record
ord-7cf7885dcbb144c0a747fa4f41c376b5
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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