HCID 23113983, compound → HCID 23114144, compound

HRID 2376286Notes

Reaction equation

HRID 2376286 reaction equation
C([NH:8][C:9]1[C:17]2[O:16][C:15]([CH3:19])([CH3:18])[C:14](=[O:20])[C:13]=2[C:12]([CH3:21])=[C:11]([CH3:22])[C:10]=1[CH3:23])C1C=CC=CC=1>C(OCC)(=O)C.CCCCCC>[NH2:8][C:9]1[C:17]2[O:16][C:15]([CH3:18])([CH3:19])[C:14](=[O:20])[C:13]=2[C:12]([CH3:21])=[C:11]([CH3:22])[C:10]=1[CH3:23]

Participants

3

Reactant 1

HCID 23113983HCID 23113983, compound

Product 1

HCID 23114144HCID 23114144, compound

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 7-(benzylamino)-2,2,4,5,6-pentamethyl-1-benzofuran-3 (2H)-one obtained in Reference Example 53, the title compound was synthesized in the same manner as in Reference Example 30. Yield: quantitative. Melting point: 141-142° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 53

Sources & evidence

ORD record
ord-fa2b8f72e893422b808d12f6edf9f908
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

Loading…