HCID 68707995, compound → HCID 68707093, compound

HRID 2376297Notes

Reaction equation

HRID 2376297 reaction equation
C([NH:8][C:9]1[CH:10]=[CH:11][C:12]2[O:16][C:15]([CH3:18])([CH3:17])[CH:14]([C:19]3[CH:24]=[CH:23][C:22]([CH:25]([CH3:27])[CH3:26])=[CH:21][CH:20]=3)[C:13]=2[CH:28]=1)C1C=CC=CC=1>CCCCCC>[CH:25]([C:22]1[CH:21]=[CH:20][C:19]([CH:14]2[C:13]3[CH:28]=[C:9]([NH2:8])[CH:10]=[CH:11][C:12]=3[O:16][C:15]2([CH3:18])[CH3:17])=[CH:24][CH:23]=1)([CH3:27])[CH3:26]

Participants

3

Reactant 1

HCID 68707995HCID 68707995, compound

Product 1

HCID 68707093HCID 68707093, compoundYield 98%

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

Using N-benzyl-3-(4-isopropylphenyl)-2,2-dimethyl-2,3-dihydro-1-benzofuran-5-amine obtained in Reference Example 85, the title compound was synthesized in the same manner as in Reference Example 30. Yield 98%. Melting point: 109-110° C. (hexane).

Workup

  1. customobtained in Reference Example 85

Sources & evidence

ORD record
ord-d48c5beac7724c3d94198a9be023f0dd
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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