HCID 86618054, compound → HCID 23113955, compound

HRID 2376323Notes

Reaction equation

HRID 2376323 reaction equation
C([O:3][C:4](=[O:25])[CH2:5][O:6][C:7]1[CH:12]=[C:11]([CH3:13])[CH:10]=[C:9]([CH3:14])[C:8]=1[CH2:15][C:16]1[CH:21]=[CH:20][C:19]([CH:22]([CH3:24])[CH3:23])=[CH:18][CH:17]=1)C>C(OCC)(=O)C.CCCCCC>[CH:22]([C:19]1[CH:18]=[CH:17][C:16]([CH2:15][C:8]2[C:9]([CH3:14])=[CH:10][C:11]([CH3:13])=[CH:12][C:7]=2[O:6][CH2:5][C:4]([OH:25])=[O:3])=[CH:21][CH:20]=1)([CH3:24])[CH3:23]

Participants

3

Reactant 1

HCID 86618054HCID 86618054, compound

Product 1

HCID 23113955HCID 23113955, compoundYield 75%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using ethyl(2-(4-isopropylbenzyl)-3,5-dimethylphenoxy)acetate obtained in Reference Example 154, the title compound was synthesized in the same manner as in Reference Example 156. Yield 75%. Melting point: 104-105° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 154

Sources & evidence

ORD record
ord-d000bcf264dc44b590956fe8a85285c8
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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