HCID 23113991, compound → HCID 23114192, compound

HRID 2376340Notes

Reaction equation

HRID 2376340 reaction equation
[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([C:8](=O)[CH2:9][O:10][C:11]2[CH:16]=[C:15]([CH3:17])[CH:14]=[C:13]([CH3:18])[C:12]=2[CH3:19])=[N:6][CH:7]=1>C(OCC)(=O)C.CCCCCC>[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[C:16]3[C:15]([CH3:17])=[CH:14][C:13]([CH3:18])=[C:12]([CH3:19])[C:11]=3[O:10][CH:9]=2)=[N:6][CH:7]=1

Participants

3

Reactant 1

HCID 23113991HCID 23113991, compound

Product 1

HCID 23114192HCID 23114192, compoundYield 87%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 1-(5-methylpyridin-2-yl)-2-(2,3,5-trimethylphenoxy)ethanone obtained in Reference Example 168, the title compound was synthesized in the same manner as in Reference Example 191. Yield 87%. Melting point: 134-135° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 168

Sources & evidence

ORD record
ord-c1ec5570d6db465cb78eb2bf7123ee05
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

Loading…