HCID 23114038, compound → HCID 23113958, compound

HRID 2376343Notes

Reaction equation

HRID 2376343 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([C:8]2[C:12]3[C:13]([CH3:19])=[CH:14][C:15]([CH3:18])=[C:16]([CH3:17])[C:11]=3[O:10][CH:9]=2)[CH:5]=[CH:6][CH:7]=1>C(OCC)(=O)C.CCCCCC>[Br:1][C:2]1[CH:3]=[C:4]([CH:8]2[C:12]3[C:13]([CH3:19])=[CH:14][C:15]([CH3:18])=[C:16]([CH3:17])[C:11]=3[O:10][CH2:9]2)[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 23114038HCID 23114038, compound

Product 1

HCID 23113958HCID 23113958, compoundYield 82%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 3-(3-bromophenyl)-4,6,7-trimethyl-1-benzofuran obtained in Reference Example 186, the title compound was synthesized in the same manner as in Reference Example 199. Yield 82%. Melting point: 73-74° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 186

Sources & evidence

ORD record
ord-320d6bb681584f6fbc425118ce1e2a74
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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