HCID 23114294, compound → HCID 23114337, compound

HRID 2376344Notes

Reaction equation

HRID 2376344 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[C:14]3[C:15]([CH3:21])=[CH:16][C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][CH:11]=2)=[C:6]([O:22][CH3:23])[CH:5]=1)([CH3:3])[CH3:2]>CO>[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH:10]2[C:14]3[C:15]([CH3:21])=[CH:16][C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][CH2:11]2)=[C:6]([O:22][CH3:23])[CH:5]=1)([CH3:3])[CH3:2]

Participants

3

Reactant 1

HCID 23114294HCID 23114294, compound

Product 1

HCID 23114337HCID 23114337, compoundYield 79%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Using 3-(4-isopropyl-2-methoxyphenyl)-4,6,7-trimethyl-1-benzofuran obtained in Reference Example 188, the title compound was synthesized in the same manner as in Reference Example 199. Yield 79%. Melting point: 102-103° C. (methanol).

Workup

  1. customobtained in Reference Example 188

Sources & evidence

ORD record
ord-c2e81527fb85436ea9278a802ea98e61
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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