HCID 23114192, compound → HCID 23114015, compound

HRID 2376346Notes

Reaction equation

HRID 2376346 reaction equation
[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[C:12]3[C:13]([CH3:19])=[CH:14][C:15]([CH3:18])=[C:16]([CH3:17])[C:11]=3[O:10][CH:9]=2)=[N:6][CH:7]=1>CO>[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([CH:8]2[C:12]3[C:13]([CH3:19])=[CH:14][C:15]([CH3:18])=[C:16]([CH3:17])[C:11]=3[O:10][CH2:9]2)=[N:6][CH:7]=1

Participants

3

Reactant 1

HCID 23114192HCID 23114192, compound

Product 1

HCID 23114015HCID 23114015, compoundYield 89%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Using 5-methyl-2-(4,6,7-trimethyl-1-benzofuran-3-yl)pyridine obtained in Reference Example 192, the title compound was synthesized in the same manner as in Reference Example 144. Yield 89%. Melting point: 69-70° C. (methanol).

Workup

  1. customobtained in Reference Example 192

Sources & evidence

ORD record
ord-7a769d88cc644aeabec101fdfad0f7f7
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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