HCID 23113870, compound → HCID 23114085, compound
Reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[C:14]3[C:15]([CH3:21])=[C:16]([CH3:20])[C:17]([CH3:19])=[CH:18][C:13]=3[O:12][CH:11]=2)=[CH:6][CH:5]=1)([CH3:3])[CH3:2]>CO>[CH:1]([C:4]1[CH:5]=[CH:6][C:7]([CH:10]2[C:14]3[C:15]([CH3:21])=[C:16]([CH3:20])[C:17]([CH3:19])=[CH:18][C:13]=3[O:12][CH2:11]2)=[CH:8][CH:9]=1)([CH3:3])[CH3:2]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
Using 3-(4-isopropylphenyl)-4,5,6-trimethyl-1-benzofuran obtained in Reference Example 194, the title compound was synthesized in the same manner as in Reference Example 199. Yield 74%. Melting point: 70-71° C. (methanol).
Workup
- customobtained in Reference Example 194
Sources & evidence
- ORD record
- ord-c9866b73af9740eca02f7a542467a963
- Source dataset
- uspto-grants-2008_12
- Patent number
- US07465815B2
Reaction notes
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