HCID 23113830, compound → HCID 23113929, compound

HRID 2376348Notes

Reaction equation

HRID 2376348 reaction equation
[C:1]([O:4][C:5]1[C:26]2[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=2)[C:8]2[O:9][CH:10]=[C:11]([C:12]3[CH:17]=[CH:16][C:15]([CH:18]([CH3:20])[CH3:19])=[CH:14][CH:13]=3)[C:7]=2[C:6]=1[CH3:27])(=[O:3])[CH3:2]>CCCCCC.C(OCC)(=O)C>[C:1]([O:4][C:5]1[C:26]2[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=2)[C:8]2[O:9][CH2:10][CH:11]([C:12]3[CH:13]=[CH:14][C:15]([CH:18]([CH3:20])[CH3:19])=[CH:16][CH:17]=3)[C:7]=2[C:6]=1[CH3:27])(=[O:3])[CH3:2]

Participants

3

Reactant 1

HCID 23113830HCID 23113830, compound

Product 1

HCID 23113929HCID 23113929, compoundYield 74%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 3-(4-isopropylphenyl)-4-methylnaphtho[1,2-b]furan-5-yl acetate obtained in Reference Example 195, the title compound was synthesized in the same manner as in Reference Example 199. Yield 74%. Melting point: 109-110° C. (hexane-ethyl acetate).

Workup

  1. customobtained in Reference Example 195

Sources & evidence

ORD record
ord-fe8a9d0302a44776a6b01b8d6dddf5f9
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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