HCID 23113893, compound → HCID 23114073, compound

HRID 2376349Notes

Reaction equation

HRID 2376349 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[C:11]3[C:22]([CH3:23])=[CH:21][C:20]4[CH2:19][CH2:18][CH2:17][CH2:16][C:15]=4[C:12]=3[O:13][CH:14]=2)=[CH:6][CH:5]=1)([CH3:3])[CH3:2]>CO>[CH:1]([C:4]1[CH:5]=[CH:6][C:7]([CH:10]2[CH2:14][O:13][C:12]3[C:15]4[CH2:16][CH2:17][CH2:18][CH2:19][C:20]=4[CH:21]=[C:22]([CH3:23])[C:11]2=3)=[CH:8][CH:9]=1)([CH3:3])[CH3:2]

Participants

3

Reactant 1

HCID 23113893HCID 23113893, compound

Product 1

HCID 23114073HCID 23114073, compoundYield 80%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Using 3-(4-isopropylphenyl)-4-methyl-6,7,8,9-tetrahydronaphtho[1,2-b]furan obtained in Reference Example 196, the title compound was synthesized in the same manner as in Reference Example 199. Yield 80%. Melting point: 54-55° C. (methanol).

Workup

  1. customobtained in Reference Example 196

Sources & evidence

ORD record
ord-a8366a7bb3264c9b8b53ce5024472833
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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