2,3,5-Trimethylphenol → HCID 68710451, compound

HRID 2376359Notes

Reaction equation

HRID 2376359 reaction equation
[CH3:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([CH3:9])=[CH:4][C:3]=1O.O[CH:12]([C:16]1[CH:21]=[CH:20][C:19]([Br:22])=[CH:18][CH:17]=1)[C:13]([OH:15])=[O:14]>C(OCC)(=O)C.CCCCCC>[Br:22][C:19]1[CH:20]=[CH:21][C:16]([CH:12]2[C:4]3[C:5]([CH3:9])=[CH:6][C:7]([CH3:8])=[C:2]([CH3:1])[C:3]=3[O:15][C:13]2=[O:14])=[CH:17][CH:18]=1

Participants

4

Reactant 2

HCID 127692,3,5-TrimethylphenolHCID 97930p-Bromomandelic acid

Product 1

HCID 68710451HCID 68710451, compoundYield 43%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 2,3,5-trimethylphenol and hydroxy(4-bromophenyl)acetic acid, the title compound was synthesized in the same manner as in Reference Example 2. Yield 43%. Melting point: 168-169° C. (ethyl acetate-hexane).

Sources & evidence

ORD record
ord-91dae15c84054f9d9eec5caf3d95e045
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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