Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromo-5-iodo-1,3-dimethylbenzene → 4-(4-Bromo-3,5-dimethyl-phenyl)-2-methoxy-pyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromo-5-iodo-1,3-dimethylbenzene | HCID 20748037 | — |
| 반응물 | (2-Methoxypyridin-4-yl)boronic acid | HCID 23546919 | — |
| 생성물 | 4-(4-Bromo-3,5-dimethyl-phenyl)-2-methoxy-pyridine | HCID 86697309 | — |
반응 단계
The title compound is prepared from 2-methoxy-pyridine-4-boronic acid and 2-bromo-5-iodo-1,3-dimethyl-benzene following a procedure analogous to that described in Step 1 of Intermediate 56. LC (method 9): tR=1.24 min; Mass spectrum (ESI+): m/z=293/295 (Br) [M+H]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08642585B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-690d248bcb1747b593004cfe50051fd6 |
| 출처 메모 | uspto-grants-2014_02 |