HCID 23113996, compound → HCID 23114254, compound

HRID 2376366Notes

Reaction equation

HRID 2376366 reaction equation
O[CH2:2][CH:3]([C:11]1[C:16]([CH3:17])=[CH:15][C:14]([CH3:18])=[C:13]([CH3:19])[C:12]=1[OH:20])[C:4]1[CH:9]=[CH:8][C:7]([Br:10])=[CH:6][CH:5]=1>CO>[Br:10][C:7]1[CH:6]=[CH:5][C:4]([CH:3]2[C:11]3[C:16]([CH3:17])=[CH:15][C:14]([CH3:18])=[C:13]([CH3:19])[C:12]=3[O:20][CH2:2]2)=[CH:9][CH:8]=1

Participants

3

Reactant 1

HCID 23113996HCID 23113996, compound

Product 1

HCID 23114254HCID 23114254, compoundYield 95%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Using 2-(2-hydroxy-1-(4-bromophenyl)ethyl)-3,5,6-trimethylphenol obtained in Reference Example 232, the title compound was synthesized in the same manner as in Reference Example 13. Yield 95%. Melting point: 72-73° C. (methanol).

Workup

  1. customobtained in Reference Example 232

Sources & evidence

ORD record
ord-fd424cb27258410193c968b1c3590f47
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

Loading…