HCID 23114037, compound → HCID 23113997, compound

HRID 2376367Notes

Reaction equation

HRID 2376367 reaction equation
[Br:1][C:2]1[C:3]([CH3:23])=[C:4]([OH:22])[C:5]([CH:10]([C:13]2[CH:18]=[CH:17][C:16]([CH:19]([CH3:21])[CH3:20])=[CH:15][CH:14]=2)[CH2:11]O)=[C:6]([CH3:9])[C:7]=1[CH3:8]>CCCCCC.C(OCC)(=O)C>[Br:1][C:2]1[C:7]([CH3:8])=[C:6]([CH3:9])[C:5]2[CH:10]([C:13]3[CH:14]=[CH:15][C:16]([CH:19]([CH3:21])[CH3:20])=[CH:17][CH:18]=3)[CH2:11][O:22][C:4]=2[C:3]=1[CH3:23]

Participants

3

Reactant 1

HCID 23114037HCID 23114037, compound

Product 1

HCID 23113997HCID 23113997, compoundYield 57%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 3-bromo-6-(2-hydroxy-1-(4-isopropylphenyl)ethyl)-2,4,5-trimethylphenol synthesized in Reference Example 234, the title compound was synthesized in the same manner as in Reference Example 13. Yield 57%. Melting point: 56-57° C. (hexane-ethyl acetate).

Workup

  1. customsynthesized in Reference Example 234

Sources & evidence

ORD record
ord-fee9b22fc71549f8b2f7e7985c288847
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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