(2,3,5-TRIMETHYLPHENOXY)ACETIC ACID → HCID 11840233, compound

HRID 2376375Notes

Reaction equation

HRID 2376375 reaction equation
[CH3:1][C:2]1[C:12]([CH3:13])=[CH:11][C:10]([CH3:14])=[CH:9][C:3]=1[O:4][CH2:5][C:6](O)=[O:7]>CCCCCC>[CH3:14][C:10]1[C:9]2[C:6](=[O:7])[CH2:5][O:4][C:3]=2[C:2]([CH3:1])=[C:12]([CH3:13])[CH:11]=1

Participants

3

Reactant 1

HCID 220046(2,3,5-TRIMETHYLPHENOXY)ACETIC ACID

Product 1

HCID 11840233HCID 11840233, compoundYield 75%

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

Using (2,3,5-trimethylphenoxy)acetic acid obtained in Reference Example 158, the title compound was synthesized in the same manner as in Reference Example 41. Yield 75%. Melting point: 92-93° C. (hexane).

Workup

  1. customobtained in Reference Example 158

Sources & evidence

ORD record
ord-11b30e46f7494b11bbb2ecb6190682f6
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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