HCID 68710656, compound → HCID 45122428, compound

HRID 2376379Notes

Reaction equation

HRID 2376379 reaction equation
C([NH:8][C:9]1[C:10]([CH3:19])=[CH:11][C:12]2[O:16][CH2:15][CH2:14][C:13]=2[C:17]=1[CH3:18])C1C=CC=CC=1>C(OCC)(=O)C.CCCCCC>[CH3:18][C:17]1[C:13]2[CH2:14][CH2:15][O:16][C:12]=2[CH:11]=[C:10]([CH3:19])[C:9]=1[NH2:8]

Participants

3

Reactant 1

HCID 68710656HCID 68710656, compound

Product 1

HCID 45122428HCID 45122428, compoundYield 86%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using N-benzyl-4,6-dimethyl-2,3-dihydro-1-benzofuran-5-amine obtained in Reference Example 270, the title compound was synthesized in the same manner as in Reference Example 30. Yield 86%. Melting point: 85-86° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 270

Sources & evidence

ORD record
ord-97b841f476d246f79e808b26cb23a493
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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