HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylpyridine-5-boronic acid → 5-(4-Bromo-3,5-dimethyl-phenyl)-2-methyl-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylpyridine-5-boronic acid | HCID 2763081 | — |
| Reactant | 2-Bromo-5-iodo-1,3-dimethylbenzene | HCID 20748037 | — |
| Product | 5-(4-Bromo-3,5-dimethyl-phenyl)-2-methyl-pyridine | HCID 86697311 | — |
Reaction Steps
The title compound is prepared from 2-methyl-pyridine-5-boronic acid and 2-bromo-5-iodo-1,3-dimethyl-benzene following a procedure analogous to that described in Step 1 of Intermediate 56. LC (method 9): tR=0.93 min; Mass spectrum (ESI+): m/z=276/278 (Br) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642585B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-f3ef43ef2dca4acd8ad53bdc9f523824 |
| Source note | uspto-grants-2014_02 |