HCID 68710442, compound → HCID 68710853, compound

HRID 2376389Notes

Reaction equation

HRID 2376389 reaction equation
C([NH:8][C:9]1[C:10]([CH3:32])=[C:11]([CH3:31])[C:12]2[O:16][CH:15]=[C:14]([C:17]3[CH:22]=[CH:21][C:20]([CH:23]4[CH2:28][CH2:27][CH2:26][CH2:25][CH2:24]4)=[CH:19][CH:18]=3)[C:13]=2[C:29]=1[CH3:30])C1C=CC=CC=1>CCCCCC>[CH:23]1([C:20]2[CH:19]=[CH:18][C:17]([C:14]3[C:13]4[C:29]([CH3:30])=[C:9]([NH2:8])[C:10]([CH3:32])=[C:11]([CH3:31])[C:12]=4[O:16][CH:15]=3)=[CH:22][CH:21]=2)[CH2:24][CH2:25][CH2:26][CH2:27][CH2:28]1

Participants

3

Reactant 1

HCID 68710442HCID 68710442, compound

Product 1

HCID 68710853HCID 68710853, compoundYield 79%

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

Using N-benzyl-3-(4-cyclohexylphenyl)-4,6,7-trimethyl-1-benzofuran-5-amine obtained in Reference Example 283, the title compound was synthesized in the same manner as in Reference Example 30. Yield 79%. Melting point: 139-140° C. (hexane).

Workup

  1. customobtained in Reference Example 283

Sources & evidence

ORD record
ord-65006e37bf4145cd901ec5b04e1796fd
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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