HCID 68709636, compound → HCID 68709490, compound

HRID 2376390Notes

Reaction equation

HRID 2376390 reaction equation
[CH2:1]([C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:13]3[C:14]([CH3:21])=[C:15]([NH2:20])[C:16]([CH3:19])=[C:17]([CH3:18])[C:12]=3[O:11][CH:10]=2)=[CH:5][CH:4]=1)[CH3:2]>CCCCCC>[CH2:1]([C:3]1[CH:8]=[CH:7][C:6]([CH:9]2[C:13]3[C:14]([CH3:21])=[C:15]([NH2:20])[C:16]([CH3:19])=[C:17]([CH3:18])[C:12]=3[O:11][CH2:10]2)=[CH:5][CH:4]=1)[CH3:2]

Participants

3

Reactant 1

HCID 68709636HCID 68709636, compound

Product 1

HCID 68709490HCID 68709490, compoundYield 80%

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

Using 3-(4-ethylphenyl)-4,6,7-trimethyl-1-benzofuran-5-amine obtained in Reference Example 311, the title compound was synthesized in the same manner as in Reference Example 144. Yield 80%. Melting point: 88-89° C. (hexane).

Workup

  1. customobtained in Reference Example 311

Sources & evidence

ORD record
ord-d21878ef5ede402b9ff736548ceb3fb6
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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