HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cumene → HCID 23113883, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cumene | HCID 7406 | — |
| Reactant | Cyclopentanecarbonyl chloride | HCID 78284 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23113883 | HCID 23113883 | — |
Reaction Steps
To a solution of cumene (16.4 g, 137 mmol) and aluminum chloride (21.9 g, 164 mmol) in dichloromethane (200 mL) was added cyclopentanecarbonyl chloride (20 g, 151 mmol) at −50° C. (the inside temperature), and the mixture was stirred for two hours until the temperature reached −10° C. (the inside temperature).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465815B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-aae28ff2a4f1424d8555cfd417950f46 |
| Source note | uspto-grants-2008_12 |