HCID 23114268, compound → HCID 23114027, compound

HRID 2376400Notes

Reaction equation

HRID 2376400 reaction equation
[CH2:1]([N:8]([C:16]1[C:21]([CH3:22])=[CH:20][C:19]([O:23]C)=[C:18]([CH2:25][C:26]2[CH:31]=[CH:30][C:29]([CH:32]([CH3:34])[CH3:33])=[CH:28][CH:27]=2)[C:17]=1[CH3:35])[C:9](=[O:15])[CH2:10][C:11]([CH3:14])([CH3:13])[CH3:12])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C(OCC)(=O)C.CCCCCC>[CH2:1]([N:8]([C:16]1[C:21]([CH3:22])=[CH:20][C:19]([OH:23])=[C:18]([CH2:25][C:26]2[CH:31]=[CH:30][C:29]([CH:32]([CH3:33])[CH3:34])=[CH:28][CH:27]=2)[C:17]=1[CH3:35])[C:9](=[O:15])[CH2:10][C:11]([CH3:12])([CH3:13])[CH3:14])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 23114268HCID 23114268, compound

Product 1

HCID 23114027HCID 23114027, compoundYield 83%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using N-benzyl-N-(3-(4-isopropylbenzyl)-4-methoxy-2,6-dimethylphenyl)-3,3-dimethylbutanamide obtained in Reference Example 332, the title compound was synthesized in the same manner as in Reference Example 335. Yield 83%. Melting point: 167-168° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 332

Sources & evidence

ORD record
ord-15e20c3d33ad41f4881a3dd1ebb468f5
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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