HCID 68710305, compound → HCID 68706938, compound

HRID 2376406Notes

Reaction equation

HRID 2376406 reaction equation
C([NH:8][C:9]1[C:10]([CH3:25])=[CH:11][C:12]2[O:16][CH2:15][CH:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)[C:13]=2[C:23]=1[CH3:24])C1C=CC=CC=1>C(OCC)(=O)C.CCCCCC>[CH3:24][C:23]1[C:13]2[CH:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)[CH2:15][O:16][C:12]=2[CH:11]=[C:10]([CH3:25])[C:9]=1[NH2:8]

Participants

3

Reactant 1

HCID 68710305HCID 68710305, compound

Product 1

HCID 68706938HCID 68706938, compoundYield 84%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using N-benzyl-4,6-dimethyl-3-phenyl-2,3-dihydro-1-benzofuran-5-amine obtained in Reference Example 357, the title compound was synthesized in the same manner as in Reference Example 30. Yield 84%. Melting point: 127-128° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 357

Sources & evidence

ORD record
ord-fd36f82024554a849e525feb9dc5920f
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

Loading…