HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxyphenylacetic Acid → HCID 68713605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxyphenylacetic Acid | HCID 7690 | — |
| Reactant | HCID 9814678 | HCID 9814678 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 68713605 | HCID 68713605 | 74% |
Reaction Steps
Using (+)-(3R)-2,2,4,6,7-pentamethyl-3-(4-methylphenyl)-2,3-dihydro-1-benzofuran-5-amine obtained in Reference Example 134 and-4-methoxyphenylacetic acid, the title compound was synthesized in the same manner as in Reference Example 359. Yield 74%. Melting point: 186-188° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465815B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-582258798b6f4d71a7622989307e1123 |
| Source note | uspto-grants-2008_12 |