HCID 68707910, compound → HCID 23114384, compound

HRID 2376410Notes

Reaction equation

HRID 2376410 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2([CH3:23])[C:14]3[C:15]([CH3:22])=[C:16]([NH2:21])[C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][CH2:11]2)=[CH:6][CH:5]=1)([CH3:3])[CH3:2]>C(OCC)(=O)C.CCCCCC>[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2([CH3:23])[C:14]3[C:15]([CH3:22])=[C:16]([NH:21][C:13](=[O:12])[CH2:14][C:10]([CH3:23])([CH3:11])[CH3:7])[C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][CH2:11]2)=[CH:6][CH:5]=1)([CH3:3])[CH3:2]

Participants

3

Reactant 1

HCID 68707910HCID 68707910, compound

Product 1

HCID 23114384HCID 23114384, compoundYield 37%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 3-(4-isopropylphenyl)-3,4,6,7-tetramethyl-2,3-dihydro-1-benzofuran-5-amine obtained in Reference Example 34, the title compound was synthesized in the same manner as in Example 1. Yield: 37%. Melting point: 194-195° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 34

Sources & evidence

ORD record
ord-1f72b155bc344df68149b94d71b404fb
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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