4-Bromo-2,6-dimethylpyridine → 4-(4-Chloro-3,5-dimethyl-phenyl)-2,6-dimethyl-pyridine

Participants

Role	Name	HCID	Charge
Reactant	4-Bromo-2,6-dimethylpyridine	HCID 13081735	—
Reactant	2-(4-Chloro-3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane	HCID 53217128	—
Product	4-(4-Chloro-3,5-dimethyl-phenyl)-2,6-dimethyl-pyridine	HCID 86697319	—

Reaction Steps

The title compound is prepared from 2-chloro-1,3-dimethyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzene and 4-bromo-2,6-dimethyl-pyridine following a procedure analogous to that described in Step 1 of Intermediate 56. Mass spectrum (ESI+): m/z=246/248 (Cl) [M+H]+.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08642585B2
Source dataset	uspto-grants-2014_02
ORD ID	ord-8293813fb18d47a48e279c41f7f0c87f
Source note	uspto-grants-2014_02