HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 23114300, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 23113846 | HCID 23113846 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 23114300 | HCID 23114300 | 42% |
Reaction Steps
Using N-(6-bromo-3-(4-isopropylphenyl)-4,7-dimethyl-2,3-dihydro-1-benzofuran-5-yl)-3,3-dimethylbutanamide obtained in Example 87 and phenylboronic acid, the title compound was synthesized in the same manner as in Example 101. Yield: 42%. Melting point: 212-213° C. (hexane-ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465815B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-9d496815c0634f8d9570722b55aef7ef |
| Source note | uspto-grants-2008_12 |