HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-N,N-dimethylaniline → HCID 11225764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-N,N-dimethylaniline | HCID 140102 | — |
| Reactant | (5-((3,3-Dimethylbutanoyl)amino)-3-(4-isopropylphenyl)-4,6-dimethyl-2,3-dihydro-1-benzofuran-7-yl)boronic acid | HCID 23114225 | — |
| Product | HCID 11225764 | HCID 11225764 | 77% |
Reaction Steps
Using (5-((3,3-dimethylbutanoyl)amino)-3-(4-isopropylphenyl)-4,6-dimethyl-2,3-dihydro-1-benzofuran-7-yl)boronic acid obtained in Example 116 and 3-bromo-N,N-dimethylaniline, the title compound was obtained in the same manner as in Example 107. Yield: 77%. Melting point: 197-199° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465815B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-7c7e288165494e31b4b010416a2c0842 |
| Source note | uspto-grants-2008_12 |