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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2376497Generated: October 30, 2026

N,N-Dimethylethylenediamine → HCID 23114344, compound

https://huagongshe.com/reaction/2376497

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN,N-DimethylethylenediamineHCID 66053—
ReactantHCID 86618058HCID 86618058—
SolventEthyl acetate hexaneHCID 21226206—
ProductHCID 23114344HCID 2311434454%

Reaction Steps

Using 2,2,2-trichloroethyl(3-(4-isopropylphenyl)-4,6,7-trimethyl-2,3-dihydro-1-benzofuran-5-yl)carbamate obtained in Example 138 and 2-(dimethylamino)ethylamine, the title compound was synthesized in the same manner as in Example 143. Yield: 54%. Melting point: 133-134° C. (hexane-ethyl acetate).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07465815B2
Source datasetuspto-grants-2008_12
ORD IDord-8acc95f77ef94fc8b8915351339d0b47
Source noteuspto-grants-2008_12