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HRID2376543

反应详情

EQUATION

反应方程式

HRID 2376543 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)CC(=O)Cl
HCID81514

Butanoyl chloride, 3,3-dimethyl-

C6H11ClO

结构：Cc1c2c(c(C(C)(O)c3ccc(C(C)C)cc3)c(C)c1NC(=O)OC(C)(C)C)OCC2
HCID86612348

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c2c(c(C(C)c3ccc(C(C)C)cc3)c(C)c1NC(=O)CC(C)(C)C)OCC2
HCID23114117

未命名化合物

收率 61%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC.CCOC(C)=O
溶剂HCID21226206

未命名化合物

PROCEDURE

实验过程

Using tert-butyl (7-(1-hydroxy-1-(4-isopropylphenyl)ethyl)-4,6-dimethyl-2,3-dihydro-1-benzofuran-5-yl)carbamate obtained in Example 223 and tert-butylacetyl chloride, the title compound was synthesized in the same manner as in Example 224. Yield: 61%. Melting point: 189-190° C. (ethyl acetate-hexane).