HCID 23114009, compound → HCID 23114366, compound

HRID 2376558Notes

Reaction equation

HRID 2376558 reaction equation
[CH2:1]([C:5]1(O)[C:9]2[CH:10]=[C:11]([NH:16][C:17](=[O:23])[CH2:18][C:19]([CH3:22])([CH3:21])[CH3:20])[C:12]([CH3:15])=[C:13]([CH3:14])[C:8]=2[O:7][C:6]1([CH3:25])[CH3:24])[CH2:2][CH2:3][CH3:4]>C(OCC)(=O)C.CCCCCC>[CH2:1]([CH:5]1[C:9]2[CH:10]=[C:11]([NH:16][C:17](=[O:23])[CH2:18][C:19]([CH3:22])([CH3:21])[CH3:20])[C:12]([CH3:15])=[C:13]([CH3:14])[C:8]=2[O:7][C:6]1([CH3:24])[CH3:25])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 1

HCID 23114009HCID 23114009, compound

Product 1

HCID 23114366HCID 23114366, compoundYield 77%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using N-(3-butyl-3-hydroxy-2,2,6,7-tetramethyl-2,3-dihydro-1-benzofuran-5-yl)-3,3-dimethylbutanamide obtained in Example 251, the title compound was synthesized in the same manner as in Example 271. Yield: 77%. Melting point: 129-130° C. (ethyl acetate-hexane).

Sources & evidence

ORD record
ord-b81dd65d13e44303a6badaf20a5ce365
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

Loading…