HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-5-methoxypyridazine → HCID 86697329, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-5-methoxypyridazine | HCID 10975612 | — |
| Reactant | 2-(4-Chloro-3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane | HCID 53217128 | — |
| Product | HCID 86697329 | HCID 86697329 | — |
Reaction Steps
The title compound is prepared from 2-chloro-1,3-dimethyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzene and 3-chloro-5-methoxy-pyridazine following a procedure analogous to that described in Step 1 of Intermediate 56. LC (method 11): tR=0.93 min; Mass spectrum (ESI+): m/z=249/251 (Cl) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642585B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-5449faba2fb54a708a93a6ab648ed7b1 |
| Source note | uspto-grants-2014_02 |