HCID 23114401, compound → HCID 23114429, compound

HRID 2376562Notes

Reaction equation

HRID 2376562 reaction equation
[CH:1]1([C:7]2(O)[C:11]3[C:12]([CH3:26])=[C:13]([NH:18][C:19](=[O:25])[CH2:20][C:21]([CH3:24])([CH3:23])[CH3:22])[C:14]([CH3:17])=[C:15]([CH3:16])[C:10]=3[O:9][C:8]2([CH3:28])[CH3:27])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1>C(OCC)(=O)C.CCCCCC>[CH:1]1([CH:7]2[C:11]3[C:12]([CH3:26])=[C:13]([NH:18][C:19](=[O:25])[CH2:20][C:21]([CH3:22])([CH3:23])[CH3:24])[C:14]([CH3:17])=[C:15]([CH3:16])[C:10]=3[O:9][C:8]2([CH3:28])[CH3:27])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1

Participants

3

Reactant 1

HCID 23114401HCID 23114401, compound

Product 1

HCID 23114429HCID 23114429, compoundYield 48%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using N-(3-cyclohexyl-3-hydroxy-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-yl)-3,3-dimethylbutanamide obtained in Example 256, the title compound was synthesized in the same manner as in Example 271. Yield: 48%. Melting point: 198-199° C. (ethyl acetate-hexane).

Sources & evidence

ORD record
ord-081b2dce0a44465989d888f920ca86db
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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