HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-chloro-m-xylene → HCID 86697331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-chloro-m-xylene | HCID 2735555 | — |
| Reactant | 3-Methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan95% | HCID 53217310 | — |
| Product | HCID 86697331 | HCID 86697331 | — |
Reaction Steps
The title compound is prepared from 3-methyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-pyridazine and 5-bromo-2-chloro-1,3-dimethyl-benzene following a procedure analogous to that described in Step 1 of Intermediate 56. LC (method 11): tR=0.91 min; Mass spectrum (ESI+): m/z=233/235 (Cl) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642585B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-24eb8852edca481ea504f986198d70e7 |
| Source note | uspto-grants-2014_02 |