HCID 23114163, compound → HCID 23113898, compound

HRID 2376581Notes

Reaction equation

HRID 2376581 reaction equation
[CH3:1][C:2]([CH3:22])([CH3:21])[CH2:3][C:4]([NH:6][C:7]1[C:8]([CH3:20])=[CH:9][C:10]2[O:14][C:13]([CH3:16])([CH3:15])[C:12](=[O:17])[C:11]=2[C:18]=1[CH3:19])=[O:5]>C1COCC1.CCCCCC>[CH3:1][C:2]([CH3:22])([CH3:21])[CH2:3][C:4]([NH:6][C:7]1[C:8]([CH3:20])=[CH:9][C:10]2[O:14][C:13]([CH3:15])([CH3:16])[CH:12]([OH:17])[C:11]=2[C:18]=1[CH3:19])=[O:5]

Participants

3

Reactant 1

HCID 23114163HCID 23114163, compound

Product 1

HCID 23113898HCID 23113898, compoundYield 82%

Reagents, catalysts & solvents 1

HCID 21883165Tetrahydrofuran hexaneSolvent

Procedure

Using 3,3-dimethyl-N-(2,2,4,6-tetramethyl-3-oxo-2,3-dihydro-1-benzofuran-5-yl)butanamide obtained in Reference Example 342, the title compound was synthesized in the same manner as in Example 234. Yield: 82%. Melting point: 217-218° C. (THF-hexane).

Workup

  1. customobtained in Reference Example 342

Sources & evidence

ORD record
ord-35985a0c2d924ba995f3e2b0151ab86a
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

Loading…