HCID 23113850, compound → HCID 23113889, compound

HRID 2376588Notes

Reaction equation

HRID 2376588 reaction equation
[CH:1]([C:4]1[CH:32]=[CH:31][C:7]([CH2:8][C:9]2[C:17]3[O:16][C:15]([CH3:19])([CH3:18])[C:14](=[O:20])[C:13]=3[C:12]([CH3:21])=[C:11]([NH:22][C:23](=[O:29])[CH2:24][C:25]([CH3:28])([CH3:27])[CH3:26])[C:10]=2[CH3:30])=[CH:6][CH:5]=1)([CH3:3])[CH3:2]>C1COCC1.CCCCCC>[OH:20][CH:14]1[C:13]2[C:12]([CH3:21])=[C:11]([NH:22][C:23](=[O:29])[CH2:24][C:25]([CH3:28])([CH3:27])[CH3:26])[C:10]([CH3:30])=[C:9]([CH2:8][C:7]3[CH:31]=[CH:32][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:5][CH:6]=3)[C:17]=2[O:16][C:15]1([CH3:19])[CH3:18]

Participants

3

Reactant 1

HCID 23113850HCID 23113850, compound

Product 1

HCID 23113889HCID 23113889, compoundYield 81%

Reagents, catalysts & solvents 1

HCID 21883165Tetrahydrofuran hexaneSolvent

Procedure

Using N-(7-(4-isopropylbenzyl)-2,2,4,6-tetramethyl-3-oxo-2,3-dihydro-1-benzofuran-5-yl)-3,3-dimethylbutanamide obtained in Reference Example 330, the title compound was synthesized in the same manner as in Example 234. Yield: 81%. Melting point: 244-245° C. (THF-hexane).

Workup

  1. customobtained in Reference Example 330

Sources & evidence

ORD record
ord-69b4c1b6124b4d179171807fe5047530
Source dataset
uspto-grants-2008_12
Patent number
US07465815B2

Reaction notes

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