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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2376589Generated: October 29, 2026

HCID 68711355, compound → HCID 68709946, compound

https://huagongshe.com/reaction/2376589

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68711355HCID 68711355—
SolventHexaneHCID 8058—
ProductHCID 68709946HCID 6870994683%

Reaction Steps

Using (cis)-3-(4-isopropylphenyl)-2,4,6,7-tetramethyl-2,3-dihydro-1-benzofuran obtained in Reference Example 352, (cis)-5-bromo-3-(4-isopropylphenyl)-2,4,6,7-tetramethyl-2,3-dihydro-1-benzofuran was synthesized in the same manner as in Reference Example 23. Using the compound, (cis)-N-benzyl-3-(4-isopropylphenyl)-2,4,6,7-tetramethyl-2,3-dihydro-1-benzofuran-5-amine was synthesized in the same manner as in Reference Example 24. Using the compound, the title compound was synthesized in the same manner as in Reference Example 30. Yield: 83%. Melting point: 91-92° C. (hexane).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07465815B2
Source datasetuspto-grants-2008_12
ORD IDord-18f3fff0579c458196ebdfac6aedfc89
Source noteuspto-grants-2008_12