HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-3-methylpyridine → HCID 86697348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-3-methylpyridine | HCID 220832 | — |
| Reactant | 2-(4-Bromo-3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane | HCID 56973136 | — |
| Product | HCID 86697348 | HCID 86697348 | — |
Reaction Steps
The title compound is prepared from 2-bromo-1,3-dimethyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzene and 2-bromo-3-methyl-pyridine following a procedure analogous to that described in Step 1 of Intermediate 56. LC (method 7): tR=0.88 min; Mass spectrum (ESI+): m/z=276/278 (Br) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642585B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-4adf818ebe9743c6be25a398fe3a5e5c |
| Source note | uspto-grants-2014_02 |