HuagongsheHuagongshe Chemistry Print Report · For research reference only
M-Cresol → (But-3-yn-1-yloxy)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | M-Cresol | HCID 342 | — |
| Reactant | Phenol | HCID 996 | — |
| Reactant | 2-Propyn-1-ol, 1-benzenesulfonate | HCID 80273 | — |
| Product | (But-3-yn-1-yloxy)benzene | HCID 9989389 | — |
Reaction Steps
The procedure for Example 614 was used, substituting 3-butynyl p-toluenesulfonate for propargyl benzenesulfonate and phenol for m-cresol to provide Example 633. 1H NMR (500 MHz, CDCl3) δ 2.02 (t, J=2 Hz, 1H), 2.68 (dt, J=8, 2 Hz, 2H), 4.08 (t, J=8 Hz, 2H), 6.96 (m, 3H), 7.30 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07468371B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-b8104ef4b95b4bb2af8c738a67af23e9 |
| Source note | uspto-grants-2008_12 |